[2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Base Information

• Chemical Name: [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane
• CAS No.: 955094-68-5
• Molecular Formula: C₃₁H₁₃Br₂Cl₈N
• Molecular Weight: 842.883
• Mol file: 955094-68-5.mol

Synonyms:[2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Chemical Property of [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

There total 2 articles about [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[4-(N-carbazolyl)-2,6-dichlorophenyl]bis(2,4,6-trichlorophenyl)methane (881917-50-6) → [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-68-5)

Guidance literature:

With N-Bromosuccinimide; silica gel; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/jo0708846

Reference yield: 33.0%

3,6-dibromo-9H-carbazole (6825-20-3) + tris(2,4,6‐trichlorophenyl)methyl radical (109745-46-2) → [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-68-5) + tris(2,4,6-trichlorophenyl)methane (105633-27-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1021/jo0708846

Reference yield: 80.0%

[2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-68-5) → [2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl (955094-74-3)

Guidance literature:

[2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane; With sodium hydroxide; In diethyl ether; dimethyl sulfoxide; at 20 ℃; for 48h;

With iodine; In diethyl ether; dimethyl sulfoxide; for 1h; Further stages.;

DOI:10.1021/jo0708846

upstream raw materials:

[4-(N-carbazolyl)-2,6-dichlorophenyl]bis(2,4,6-trichlorophenyl)methane

3,6-dibromo-9H-carbazole

tris(2,4,6‐trichlorophenyl)methyl radical

Downstream raw materials:

[2,6-dichloro-4-(3,6-dibromo-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl