trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester
CAS No.:851594-63-3
Molecular Formula:C₁₅H₉F₃O₆S
Molecular Weight:374.294
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

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Chemical Property of trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

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Technology Process of trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

There total 5 articles about trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851594-70-2
2-{(2R,6S)-6-[(2R,4R,5S)-7-((2S,6R)-6-Allyl-tetrahydro-pyran-2-yl)-2-(tert-butyl-dimethyl-silanyloxy)-4-hydroxy-5-methyl-heptyl]-tetrahydro-pyran-2-yl}-2-methyl-propionic acid benzyl ester

: 851594-63-3
trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 4 h / 20 °C / Photolysis

2: 30 percent / 4-(dimethylamino)pyridine; thionyl chloride / 1,2-dimethoxy-ethane / 0 - 20 °C

3: 95 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; dmap; thionyl chloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/anie.200462577

Reference yield:

: 851594-67-7
3-(tert-butyldimethylsilanyloxy)-2,2-dimethyl-1-phenylpropan-1-ol

: 851594-63-3
trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 4 h / 20 °C / Photolysis

2: 30 percent / 4-(dimethylamino)pyridine; thionyl chloride / 1,2-dimethoxy-ethane / 0 - 20 °C

3: 95 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; dmap; thionyl chloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/anie.200462577

Reference yield:

: 303-07-1
2,6-Dihydroxybenzoic acid

: 851594-63-3
trifluoromethanesulfonic acid 4-oxo-2-phenyl-4H-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / 4-(dimethylamino)pyridine; thionyl chloride / 1,2-dimethoxy-ethane / 0 - 20 °C

2: 95 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; dmap; thionyl chloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/anie.200462577