(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

Base Information

Chemical Name:(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)
CAS No.:71272-82-7
Molecular Formula:C₃₈H₃₆Cl₄P₂Ru₂
Molecular Weight:898.603
Hs Code.:

Synonyms:(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

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Chemical Property of (μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

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Technology Process of (μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

There total 3 articles about (μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: 71272-82-7
(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

Guidance literature:: With Ph₂PCH₂CH₂PPh₂; In benzene; N2 atmosphere; equimolar amts., refluxing for 2 h (pptn.); collection, washing (C6H6), crystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1016/S0020-1693(00)94652-8

Reference yield:

: 69058-50-0
RuCl₂(C₆H₆)(CH₃S(O)CH₃)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 71272-82-7
(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

Guidance literature:: In dichloromethane; byproducts: Me2SO; half an equiv of diphosphine is added to the Ru complex in CH2Cl2 at room temp.; elem. anal.;
DOI:10.1016/0022-328X(93)83387-B

Reference yield:

: 69058-50-0
RuCl₂(C₆H₆)(CH₃S(O)CH₃)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: trans-RuCl₂(1,2-bis(diphenylphosphino)ethane)₂

: 71272-85-0
(η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride

: 71272-82-7
(μ-1,2-bis(diphenylphosphino)ethane)bis(η(6)-benzene)tetrachlorodiruthenium(II)

Guidance literature:: In methanol; dichloromethane; react. of the Ru complex with one equiv of the diphosphine in CH2Cl2-MeOH at room temp.; elem. anal.;
DOI:10.1016/0022-328X(93)83387-B