(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

Base Information

Chemical Name:(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate
CAS No.:610784-26-4
Molecular Formula:C₂₇H₄₄N₂O₄S
Molecular Weight:492.723
Hs Code.:

Synonyms:(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

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Technology Process of (2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

There total 2 articles about (2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 57244-09-4
2-Cyanobutanoyl chloride

: 610784-26-4
(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

Guidance literature:: With silver cyanide; In toluene; at 80 ℃; for 4h;
DOI:10.1021/jo00088a034

Reference yield:

: 51789-75-4
1-cyano-propane-1-carboxylic acid

: 610784-26-4
(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅

2: 91 percent / AgCN / toluene / 4 h / 80 °C

With silver cyanide; phosphorus pentachloride; In toluene;
DOI:10.1021/jo00088a034

Reference yield: 68.0%

: 620-05-3
iodomethylbenzene

: 610784-26-4
(2RS)-(1'S,2'R,4'R)-10'-(dicyclohexylsulfamoyl)isobornyl-2-cyanobutanoate

: 154520-15-7
(2S)-(1S,2R,4R)-10-(Dicyclohexylsulfamoyl)isobornyl 2-benzyl-2-cyanobutanoate

: (2R)-(1S,2R,4R)-10-(Dicyclohexylsulfamoyl)isobornyl 2-benzyl-2-cyanobutanoate

Guidance literature:: With lithium diisopropyl amide; Yields of byproduct given; 1.) THF, -78 deg C, 1 h, 2.) THF, HMPA, -78 deg C to r.t.; r.t., 1 d;
DOI:10.1021/jo00088a034