2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:881209-85-4
Molecular Formula:C₄₀H₇₃BO₄
Molecular Weight:628.828
Hs Code.:

Synonyms:2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about 2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 881209-76-3
4-bromo-1,2-bis(tetradecyloxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 881209-85-4
2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 90 ℃; for 24h; Inert atmosphere; Alkaline conditions;
DOI:10.1002/asia.202100173

Reference yield:

: C₃₆H₆₇BO₄

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 881209-85-4
2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: C₃₆H₆₇BO₄; 2,3-dimethyl-2,3-butane diol; In tetrahydrofuran; hexane; at 20 ℃; for 2h;

With acetic acid; In tetrahydrofuran; hexane; at 20 ℃; for 18h;
DOI:10.1002/chem.200500903

Reference yield:

: 881209-76-3
4-bromo-1,2-bis(tetradecyloxy)benzene

: 881209-85-4
2-[3,4-bis(tetradecyloxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / -78 °C

1.2: hexane; tetrahydrofuran / 2.5 h / -78 - 20 °C

2.1: hexane; tetrahydrofuran / 2 h / 20 °C

2.2: glacial acetic acid / hexane; tetrahydrofuran / 18 h / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/chem.200500903