Technology Process of C20H24O3Se
There total 5 articles about C20H24O3Se which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
tetrahydrofuran;
0 deg C, 0.5 h, room temperature, 5 h;
DOI:10.1021/jo9613085
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) iodine, potassium iodide, NaHCO3, 2.) DIBALH / 1.) CH2Cl2, H2O, 0 deg C, 1.5 h, 2.) THF, hexane, -78 deg C, 0.5 h
2: 92 percent / NaH / dimethylformamide / 0.25 h / 0 °C
3: 98 percent / NaBH4 / ethanol / 1 h / Ambient temperature
4: 90 percent / H2O2 / tetrahydrofuran / 0 deg C, 0.5 h, room temperature, 5 h
With
sodium tetrahydroborate; dihydrogen peroxide; iodine; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium iodide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo9613085
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / NaH / dimethylformamide / 0.25 h / 0 °C
2: 98 percent / NaBH4 / ethanol / 1 h / Ambient temperature
3: 90 percent / H2O2 / tetrahydrofuran / 0 deg C, 0.5 h, room temperature, 5 h
With
sodium tetrahydroborate; dihydrogen peroxide; sodium hydride;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo9613085