Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

Base Information

Chemical Name:Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester
CAS No.:214068-96-9
Molecular Formula:C₃₂H₅₆NO₆P
Molecular Weight:581.773
Hs Code.:

Synonyms:Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

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Chemical Property of Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

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Technology Process of Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

There total 2 articles about Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 128753-68-4
(benzyloxy)chloro(diisopropylamino)phosphane

: 113973-38-9
sn-2,3-dioctanoylglycerol

: 214068-96-9
Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jo980501r

Reference yield:

: 214068-80-1
Octanoic acid (R)-2-(4-methoxy-benzyloxy)-1-octanoyloxymethyl-ethyl ester

: 214068-96-9
Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DDQ / CH₂Cl₂; H₂O / 3 h / Ambient temperature

2: 89 percent / i-Pr₂NEt / CH₂Cl₂ / 2 h / 0 °C

With N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1021/jo980501r

Reference yield:

: 214068-96-9
Octanoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octanoyloxymethyl-ethyl ester

: C₂₅H₄₅O₁₆P₂^(3-)*3Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: 4,5-dicyanoimidazole / toluene; CH₂Cl₂

2: aq. H₂O₂ / toluene; CH₂Cl₂

3: 85 percent / H₂; NaHCO₃ / Pd(OH)2/C / 2-methyl-propan-2-ol; H₂O

With 4,5-dicyano-1H-imidazole; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate; palladium dihydroxide; In dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/jo060702s