(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

Base Information

Chemical Name:(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester
CAS No.:152036-25-4
Molecular Formula:C₂₁H₃₂N₂O₄
Molecular Weight:376.496
Hs Code.:

Synonyms:(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

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Chemical Property of (2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

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Technology Process of (2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

There total 3 articles about (2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 152036-17-4
(2S,5S)-3-Methyl-4-oxo-5-(phenylacetyl)imidazolidin-1-carbonsaeure-t-butylester

: 152036-25-4
(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at -10 ℃; for 3h;

Reference yield:

: 119838-38-9
(2S)-1-(tert-butyloxycarbonyl)-2-tert-butyl-3-methylimidazolidin-4-one

: 152036-25-4
(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) iPr₂NLi / 1) THF, 30 min, -78 deg C, 2) THF, 1 h, -100 deg C

2: 21 percent / LiBHEt₃ / tetrahydrofuran / 3 h / -10 °C

With lithium triethylborohydride; lithium diisopropyl amide; In tetrahydrofuran;

Reference yield:

: 103-80-0
phenylacetyl chloride

: 152036-25-4
(2S,5S,1'S)-5-(1'-Hydroxy-2'-phenylethyl)-3-methyl-4-oxoimidazolidin-1-carbonsaeure-t-butylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) iPr₂NLi / 1) THF, 30 min, -78 deg C, 2) THF, 1 h, -100 deg C

2: 21 percent / LiBHEt₃ / tetrahydrofuran / 3 h / -10 °C

With lithium triethylborohydride; lithium diisopropyl amide; In tetrahydrofuran;