1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

Base Information

Chemical Name:1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine
CAS No.:791097-00-2
Molecular Formula:C₅₁H₅₄N₂O₅
Molecular Weight:775
Hs Code.:

Synonyms:1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

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Chemical Property of 1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

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Technology Process of 1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

There total 7 articles about 1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: 791096-99-6
Acetic acid (2S,3S,4R,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(1,3-dibenzyl-imidazolidin-2-yl)-tetrahydro-pyran-3-yl ester

: 791097-00-2
1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

Guidance literature:: Acetic acid (2S,3S,4R,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(1,3-dibenzyl-imidazolidin-2-yl)-tetrahydro-pyran-3-yl ester; With sodium methylate; In methanol;

benzyl bromide; With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2004.08.034

Reference yield:

: 215510-13-7
1-(β-D-glucopyranosyl)propan-2-one

: 791097-00-2
1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 91 percent / pyridine

2.1: NaI; pyridine / acetonitrile; pentane / 12 h / 52 °C

3.1: dimethyldioxirane; K₂CO₃ / acetone

3.2: aq. HCl / tetrahydrofuran

4.1: NaIO₄ / tetrahydrofuran; H₂O

5.1: toluene

6.1: NaOMe / methanol

6.2: 90 percent / NaH / dimethylformamide

With pyridine; sodium periodate; sodium methylate; 3,3-dimethyldioxirane; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; water; acetone; toluene; acetonitrile; pentane;
DOI:10.1016/j.tetlet.2004.08.034

Reference yield:

: 469873-50-5
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)propane-2-one

: 791097-00-2
1,3-Dibenzyl-2-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-imidazolidine

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaI; pyridine / acetonitrile; pentane / 12 h / 52 °C

2.1: dimethyldioxirane; K₂CO₃ / acetone

2.2: aq. HCl / tetrahydrofuran

3.1: NaIO₄ / tetrahydrofuran; H₂O

4.1: toluene

5.1: NaOMe / methanol

5.2: 90 percent / NaH / dimethylformamide

With pyridine; sodium periodate; sodium methylate; 3,3-dimethyldioxirane; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; water; acetone; toluene; acetonitrile; pentane;
DOI:10.1016/j.tetlet.2004.08.034