N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline
CAS No.:873656-95-2
Molecular Formula:C₂₂H₃₅NO₄Si
Molecular Weight:405.61
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

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Chemical Property of N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

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Technology Process of N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

There total 1 articles about N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1-(tert-butyldimethylsiloxy)-2-(tributylstannyl)-2,3-butadiene

: 157496-75-8
tert-butyl (2-iodo-4-methoxyphenyl)carbamate

: 873656-95-2
N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

Guidance literature:: With copper(l) iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; trifuran-2-yl-phosphane; In N,N-dimethyl-formamide; at 50 ℃; for 3h;
DOI:10.1021/ol052179u

Reference yield:

: 873656-95-2
N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

: 958882-91-2
[2-(1-hydroxymethyl-propa-1,2-dienyl)-4-methoxy-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/ol060418n

Reference yield:

: 873656-95-2
N-(tert-butoxycarbonyl)-2-[1-(tert-butyldimethylsiloxy)-2,3-butadien-2-yl]-4-methoxyaniline

: 888732-09-0
2-(1-acetoxy-2,3-butadien-2-yl)-N-(tert-butoxycarbonyl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH; TBAF / tetrahydrofuran / 3 h / 0 °C

2: pyridine / 1 h / 0 °C

With pyridine; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran;
DOI:10.1021/ol060418n