Tert-butyl 2-iodo-4-methoxyphenylcarbamate

Base Information

Chemical Name:Tert-butyl 2-iodo-4-methoxyphenylcarbamate
CAS No.:157496-75-8
Molecular Formula:C12H16INO3
Molecular Weight:349.168
Hs Code.:
DSSTox Substance ID:DTXSID60356055
Nikkaji Number:J669.309A
Wikidata:Q82135191
Mol file:157496-75-8.mol

Synonyms:tert-butyl 2-iodo-4-methoxyphenylcarbamate;157496-75-8;tert-butyl (2-iodo-4-methoxyphenyl)carbamate;tert-butyl N-(2-iodo-4-methoxyphenyl)carbamate;DTXSID60356055;QVVBFDVJTIYVAU-UHFFFAOYSA-N;AB6709;MFCD04971380;SB83549;tert-butyl(2-iodo-4-methoxyphenyl)carbamate;CS-0328638;EN300-5007716;AI-942/42302123;J-524448

Suppliers and Price of Tert-butyl 2-iodo-4-methoxyphenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(2-iodo-4-methoxyphenyl)carbamate 95+%
1g
$ 395.00

Crysdot
tert-Butyl(2-iodo-4-methoxyphenyl)carbamate 95+%
5g
$ 1584.00

Chemcia Scientific
(2-Iodo-4-methoxy-phenyl)-carbamicacidtert-butylester 95%
5 G
$ 1050.00

American Custom Chemicals Corporation
TERT-BUTYL-2-IODO-4-METHOXYPHENYLCARBAMATE 95.00%
5MG
$ 502.71

Total 6 raw suppliers

Chemical Property of Tert-butyl 2-iodo-4-methoxyphenylcarbamate

Chemical Property:

Melting Point:49-50 °C
Boiling Point:341.8±32.0 °C(Predicted)
PKA:12.48±0.70(Predicted)
PSA：47.56000
Density:1.555±0.06 g/cm3(Predicted)
LogP:3.71980
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:349.01749
Heavy Atom Count:17
Complexity:265

Purity/Quality:

95% ^*data from raw suppliers

tert-Butyl(2-iodo-4-methoxyphenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC1=C(C=C(C=C1)OC)I

Technology Process of Tert-butyl 2-iodo-4-methoxyphenylcarbamate

There total 11 articles about Tert-butyl 2-iodo-4-methoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 191348-14-8
2-iodo-4-methoxylaniline

: 157496-75-8
tert-butyl (2-iodo-4-methoxyphenyl)carbamate

Guidance literature:: In tetrahydrofuran; for 48h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.06.027

Reference yield: 86.0%

: 18437-68-8
tert-butyl N-(4-methoxyphenyl)carbamate

: 157496-75-8
tert-butyl (2-iodo-4-methoxyphenyl)carbamate

Guidance literature:: tert-butyl N-(4-methoxyphenyl)carbamate; With tert.-butyl lithium; In diethyl ether;

With 1,2-Diiodoethane; In diethyl ether; at -78 - 20 ℃; Further stages.;
DOI:10.1039/b108622g