7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene

Base Information

• Chemical Name: 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene
• CAS No.: 433961-34-3
• Molecular Formula: C₇₈H₈₈N₄O₁₀
• Molecular Weight: 1241.58

Synonyms:7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene

Chemical Property of 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene

Chemical Property:

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Technology Process of 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene

There total 2 articles about 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.8%

N-butylamine (109-73-9,85404-21-3) + C70H68O14 (251323-68-9,571145-04-5) → 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene (433961-34-3)

Guidance literature:

In ethanol; for 168h; Heating;

DOI:10.1021/jo011138i

Reference yield:

7,13,21,27-tetraphenyl-29,30,31,32-tetrahydroxy-2,3,16,17-tetrahomo-3,17-dioxacalix[4]arene → 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene (433961-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate

2: 85.8 percent / ethanol / 168 h / Heating

With potassium carbonate; In ethanol;

DOI:10.1021/jo011138i

Reference yield: 76.2%

7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(butylcarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene (433961-34-3) → 7,13,21,27-tetraphenyl-29,30,31,32-tetrakis(N-butylthiocarbamoyl)methoxy-2,3-16,17-tetrahomo-3,17-dioxacalix[4]arene

Guidance literature:

With Lawessons reagent; In toluene; at 90 ℃; for 20h;

DOI:10.1021/jo011138i

upstream raw materials:

N-butylamine

C₇₀H₆₈O₁₄

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