3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

Base Information

Chemical Name:3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt
CAS No.:914775-75-0
Molecular Formula:C₁₄H₁₈FO₄*Li
Molecular Weight:276.234
Hs Code.:

Synonyms:3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

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Chemical Property of 3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

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Technology Process of 3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

There total 2 articles about 3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 914775-74-9
1-tert-butyl-5-fluoro-2-methoxymethoxy-4-methylbenzene

: 124-38-9,18923-20-1
carbon dioxide

: 914775-75-0
3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

Guidance literature:: 1-tert-butyl-5-fluoro-2-methoxymethoxy-4-methylbenzene; With n-butyllithium; In tetrahydrofuran; at -78 - 0 ℃; for 1.58333h;

carbon dioxide; In tetrahydrofuran; for 0.0833333h;

Reference yield:

: 220901-47-3
2-tert-butyl-4-fluoro-5-methylphenol

: 914775-75-0
3-tert-butyl-5-fluoro-2-methoxymethoxy-6-methylbenzoic acid, lithium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexachloroethane / 1.5 h / -78 - 0 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexachloroethane;