O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

Base Information

Chemical Name:O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine
CAS No.:112924-70-6
Molecular Formula:C₄₁H₄₃NO₅
Molecular Weight:629.796
Hs Code.:

Synonyms:O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

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Chemical Property of O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

Chemical Property:

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Technology Process of O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

There total 8 articles about O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: imidazole-1-carbothioic acid O-[(1R,2R,3R,4S)-2,3,4-tris-benzyloxy-5-benzyloxyimino-1-benzyloxymethyl]pentyl ester

: 112924-70-6
O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

: 112684-57-8
O-benzyl-N-[(1R,2S,3S,4R,5R)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 4h; Heating;
DOI:10.1039/b315704k

Reference yield: 39.0%

: 112684-52-3
thiocarbonic acid O-phenyl ester O-(2,3,4-tris-benzyloxy-5-benzyloxyimino-1-benzyloxymethyl-pentyl) ester

: 112924-70-6
O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

: 112684-57-8
O-benzyl-N-[(1R,2S,3S,4R,5R)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 4h; Heating;
DOI:10.1021/ol991252b

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 112924-70-6
O-benzyl-N-[(1R,2S,3S,4R,5S)-2,3,4-tris-benzyloxy-5-benzyloxymethylcyclopentyl]-N-hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / methanol; pyridine / 3.5 h / 90 °C

2: 73 percent / pyridine / CH₂Cl₂ / 3.5 h / 0 °C

3: 27 percent / Bu₃SnH; AIBN / benzene / 4 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In pyridine; methanol; dichloromethane; benzene; 1: Condensation / 2: Condensation / 3: Cyclization;
DOI:10.1021/ol991252b