2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

Base Information

Chemical Name:2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate
CAS No.:124575-24-2
Molecular Formula:C₃₂H₃₇N₂O₁₀P
Molecular Weight:640.627
Hs Code.:

Synonyms:2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

There total 11 articles about 2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₇N₂O₉P

: 124575-24-2
2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

Guidance literature:: With dihydrogen peroxide; In dichloromethane; water; acetonitrile; at 0 ℃; for 0.75h;
DOI:10.3987/COM-18-S(T)50

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 124575-24-2
2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / TMSN₃ / SnCl₄ / CH₂Cl₂

2: 1.) H₂; 2.) DCC / 1.) PtO₂ / 1.) acetone

3: 2.) Dowex 50W-X₈ / 1.) NaOMe / 1.) MeOH

4: Dowex 50W-X₈ / acetone

5: 1.) 1H-tetrazole; 2.) m-CPBA / 1.) CH₂Cl₂

With 1H-tetrazole; trimethylsilylazide; Dowex 50W-X₈; hydrogen; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; platinum(IV) oxide; sodium methylate; tin(IV) chloride; In dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)99530-3

Reference yield:

: 103268-51-5
C₃₆H₃₂N₂O₁₀

: 124575-24-2
2,3-O-isopropylidene-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine-5-dibenzylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) Dowex 50W-X₈ / 1.) NaOMe / 1.) MeOH

2: Dowex 50W-X₈ / acetone

3: 1.) 1H-tetrazole; 2.) m-CPBA / 1.) CH₂Cl₂

With 1H-tetrazole; Dowex 50W-X₈; 3-chloro-benzenecarboperoxoic acid; sodium methylate; In acetone;
DOI:10.1016/S0040-4039(00)99530-3