2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

Base Information

Chemical Name:2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine
CAS No.:63621-56-7
Molecular Formula:C₁₈H₂₄N₂O₇
Molecular Weight:380.398
Hs Code.:

Synonyms:2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

There total 10 articles about 2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₂₀H₂₆N₂O₈

: 63621-57-8
2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

: 63621-56-7
2,3-O-isopropylidene-5-hydroxy-1-N-(benzyloxycarbonylglycyl)-D-ribofuranosylamine

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 0.5h;
DOI:10.3987/COM-18-S(T)50

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 63621-56-7,63621-57-8
[((3aR,6R,6aR)-6-Hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl)-methyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / TMSN₃ / SnCl₄ / CH₂Cl₂

2: 1.) H₂; 2.) DCC / 1.) PtO₂ / 1.) acetone

3: 2.) Dowex 50W-X₈ / 1.) NaOMe / 1.) MeOH

4: Dowex 50W-X₈ / acetone

With trimethylsilylazide; Dowex 50W-X₈; hydrogen; dicyclohexyl-carbodiimide; platinum(IV) oxide; sodium methylate; tin(IV) chloride; In dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)99530-3

Reference yield:

: 103268-51-5
C₃₆H₃₂N₂O₁₀

: 63621-56-7,63621-57-8
[((3aR,6R,6aR)-6-Hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl)-methyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Dowex 50W-X₈ / 1.) NaOMe / 1.) MeOH

2: Dowex 50W-X₈ / acetone

With Dowex 50W-X₈; sodium methylate; In acetone;
DOI:10.1016/S0040-4039(00)99530-3