tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate

Base Information

• Chemical Name: tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate
• CAS No.: 1187972-08-2
• Molecular Formula: C₃₀H₄₃NO₇
• Molecular Weight: 529.674

Synonyms:tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate

Chemical Property of tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate

Chemical Property:

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Technology Process of tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate

There total 1 articles about tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-6-hydroxy-3-(triethylsilyloxy)hexyl]-2,2-dimethyloxazolidine-3-carboxylate (1187972-07-1) → tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate (1187972-08-2)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.75h; Inert atmosphere;

DOI:10.1016/j.tet.2009.06.046

Reference yield:

tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-3,6-dihydroxyhexyl]-2,2-dimethyloxazolidine-3-carboxylate (1187972-08-2) + methanesulfonyl chloride (124-63-0) → C32H47NO11S2

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tet.2009.06.046

upstream raw materials:

tert-butyl (R)-4-[(1R,2S,3S)-1,2-bis(benzyloxy)-6-hydroxy-3-(triethylsilyloxy)hexyl]-2,2-dimethyloxazolidine-3-carboxylate

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