1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

Base Information

Chemical Name:1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane
CAS No.:154519-99-0
Molecular Formula:C₂₆H₁₈BrF₃O₃
Molecular Weight:515.326
Hs Code.:

Synonyms:1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

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Technology Process of 1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

There total 1 articles about 1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 154519-97-8
4-(4-Bromophenoxy)trifluoroacetophenone

: 108-95-2,27073-41-2
phenol

: 154519-99-0
1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

Guidance literature:: trifluorormethanesulfonic acid; at 100 ℃; for 72h;
DOI:10.1021/jo00088a035

Reference yield: 83.0%

: 536-74-3
phenylacetylene

: 154519-99-0
1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

: 1,1-Bis(4-hydroxyphenyl)-1-<4-<4-(phenylethynyl)phenoxy>phenyl>-2,2,2-trifluoroethane

Guidance literature:: With copper(l) iodide; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In triethylamine; at 90 ℃; for 48h;
DOI:10.1021/jo00088a035

Reference yield:

: 154519-99-0
1,1-Bis(4-hydroxyphenyl)-1-<4-(4-bromophenoxy)phenyl>-2,2,2-trifluoroethane

: 1,1-Bis(4-hydroxyphenyl)-1-<4-(4-ethynylphenoxy)phenyl>-2,2,2-trifluoroethane

Guidance literature:: Multi-step reaction with 2 steps

1: CuI, Ph₃P / (Ph₃P)4Pd⁽⁰⁾ / various solvent(s)

2: desilylation

With copper(l) iodide; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In various solvent(s);
DOI:10.1021/jo00088a035