benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

Base Information

Chemical Name:benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide
CAS No.:786709-28-2
Molecular Formula:C₁₄H₁₇NO₃S
Molecular Weight:279.36
Hs Code.:

benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ<sup>4</sup>,2-thiazine-2-carboxylate 1-oxide

Synonyms:benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

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Chemical Property of benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

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Technology Process of benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

There total 1 articles about benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5194-51-4
(2E,4E)-hexa-2,4-diene

: 86120-34-5
N-sulfinyl benzyl carbamate

: benzyl (1R,3S,6R)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

: 786709-28-2
benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); In dichloromethane; at -45 ℃; for 24h; Title compound not separated from byproducts;
DOI:10.1021/jo0490245

Reference yield:

: 786709-28-2
benzyl (1S,3R,6S)-3,6-dihydro-3,6-dimethyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

: 28819-05-8,64562-95-4,67799-99-9
N-benzyloxycarbonyl-D-alanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / -60 °C

2: NaOH; O₃ / -78 - 20 °C

With sodium hydroxide; ozone; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo0490245