N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine

Base Information

• Chemical Name: N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine
• CAS No.: 326913-70-6
• Molecular Formula: C₂₁H₁₇N₃OS
• Molecular Weight: 359.451

Synonyms:N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine

Chemical Property of N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine

Chemical Property:

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Technology Process of N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine

There total 3 articles about N²-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N⁴-naphthalen-2-yl-thiazole-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ortho-anisaldehyde (135-02-4) + β-(2-amino-thiazol-4-yl)aminonaphthalene (326913-65-9) → N2-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N4-naphthalen-2-yl-thiazole-2,4-diamine (326913-70-6)

Guidance literature:

In acetic acid; for 16h; Heating;

Reference yield:

naphthalen-2-ylamine (91-59-8) → N2-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N4-naphthalen-2-yl-thiazole-2,4-diamine (326913-70-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / ethanol

2: 60 percent / ethanol / 10 h / Heating

3: 50 percent / acetic acid / 16 h / Heating

In ethanol; acetic acid;

Reference yield:

N-(2-naphthyl)-2-chloroacetamide (5453-65-6) → N2-[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-N4-naphthalen-2-yl-thiazole-2,4-diamine (326913-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / ethanol / 10 h / Heating

2: 50 percent / acetic acid / 16 h / Heating

In ethanol; acetic acid;

upstream raw materials:

ortho-anisaldehyde

β-(2-amino-thiazol-4-yl)aminonaphthalene

naphthalen-2-ylamine

N-(2-naphthyl)-2-chloroacetamide

Downstream raw materials:

C₂₇H₂₁N₅OS

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