[3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III)

Base Information

• Chemical Name: [3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III)
• CAS No.: 1450643-81-8
• Molecular Formula: C₂₆H₂₃ClF₃O₆RhS
• Molecular Weight: 658.885

Synonyms:[3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III)

Chemical Property of [3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III)

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Technology Process of [3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III)

There total 1 articles about [3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η⁵-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer + silver trifluoromethanesulfonate (2923-28-6) + 3-Hydroxy-4'-chloroflavone (19275-70-8) → [3-(oxo-κO)-2-(4-chlorophenyl)-chromen-4-onato-κO](η5-pentamethylcyclopentadienyl)(trifluoromethanesulfonato-κO)rhodium(III) (1450643-81-8)

Guidance literature:

With sodium methylate; In methanol; for 18h; Reflux; Inert atmosphere;

DOI:10.1002/zaac.201300145

upstream raw materials:

silver trifluoromethanesulfonate

3-Hydroxy-4'-chloroflavone

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