C₂₃H₂₄F₃NO₂S

Base Information

Chemical Name:C₂₃H₂₄F₃NO₂S
CAS No.:1415576-72-5
Molecular Formula:C₂₃H₂₄F₃NO₂S
Molecular Weight:435.51
Hs Code.:

C<sub>23</sub>H<sub>24</sub>F<sub>3</sub>NO<sub>2</sub>S

Synonyms:C₂₃H₂₄F₃NO₂S

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Chemical Property of C₂₃H₂₄F₃NO₂S

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Technology Process of C₂₃H₂₄F₃NO₂S

There total 5 articles about C₂₃H₂₄F₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415577-69-3
C₁₅H₁₆F₃NO₂S

: 823213-29-2
C₂₄H₂₇BiCl₂

: 1415576-72-5
C₂₃H₂₄F₃NO₂S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; toluene; at 10 - 30 ℃; for 12h; Inert atmosphere;

Reference yield:

: 76041-72-0
2-mercapto-5-trifluoromethylpyridine

: 1415576-72-5
C₂₃H₂₄F₃NO₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrahydrofuran / 1.5 h / 0 °C / Cooling with ice

2.1: chloroform / 8 h / 0 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

3.2: 0.5 h / Reflux

4.1: water; sodium carbonate / 5 h / Reflux

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform; toluene / 12 h / 10 - 30 °C / Inert atmosphere

With water; sodium methylate; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; chloroform; toluene; 2.1: |Wittig Olefination;

Reference yield:

: 1415577-68-2
C₁₇H₁₇F₃NO₄S^(1-)*Na⁽¹⁺⁾

: 1415576-72-5
C₂₃H₂₄F₃NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium carbonate / 5 h / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform; toluene / 12 h / 10 - 30 °C / Inert atmosphere

With water; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; toluene;