N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

Base Information

Chemical Name:N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide
CAS No.:1391595-64-4
Molecular Formula:C₃₂H₃₂N₄O₂S
Molecular Weight:536.698
Hs Code.:

Synonyms:N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

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Technology Process of N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

There total 7 articles about N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1391595-58-6
N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylmesylate

: 1391595-64-4
N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/cbic.201200579

Reference yield:

: 1404291-74-2
N-(Boc)-S-trityl-3-amino-4-(mercaptomethyl)benzyl alcohol

: 1391595-64-4
N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With sodium azide; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cbic.201200579

Reference yield:

: 1391595-57-5
methyl 3-((tert-butoxycarbonyl)amino)-4-((tritylthio)methyl)benzoate

: 1391595-64-4
N-boc-S-trityl-3-amino-4-(mercaptomethyl)benzylazide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cbic.201200579