methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

Base Information

Chemical Name:methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate
CAS No.:134915-82-5
Molecular Formula:C₂₄H₂₇N₃O₆
Molecular Weight:453.495
Hs Code.:

Synonyms:methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

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Chemical Property of methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

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Technology Process of methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

There total 3 articles about methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55355-50-5
N^ω-benzyloxycarbonyl-(RS)-lysine methyl ester hydrochloride

: 134915-82-5
methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄, Et₃N / CH₂Cl₂

With magnesium sulfate; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)79701-2

Reference yield:

: 5332-26-3
N-(bromomethyl)phtalimide

: N^α-(4-chlorobenzylidene)-N^ε-benzyloxycarbonyl-(RS)-lysine methyl ester

: 134915-82-5
methyl (RS)-2-amino-6-benzyloxycarbonylamino-2-phthalimidomethylhexanoate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 1 h; 2.) THF, hexane, -70 deg C, 40 min then r.t., 20 h;
DOI:10.1016/0040-4020(95)00273-B