Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

Base Information

Chemical Name:Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate
CAS No.:105199-40-4
Molecular Formula:C₂₁H₁₉N₂O₃S*Na
Molecular Weight:402.449
Hs Code.:

Synonyms:Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

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Chemical Property of Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

There total 1 articles about Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7357-70-2
Cyanothioacetamide

: 17451-18-2,39626-31-8,125105-17-1
(Z)-2-benzoyl-3-phenylacrylic acid ethyl ester

: 105199-40-4
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;

Reference yield: 75.0%

: 105199-40-4
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

: 105199-50-6
5-Cyano-2,4-diphenyl-6-thioxo-1,4,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester

Guidance literature:: With acetic acid; In water;

Reference yield:

: 105199-40-4
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

: 105199-60-8
4,6-Diphenyl-5-ethoxycarbonyl-3-cyanopyridine-2(1H)thione

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / acetic acid / H₂O

2: 77 percent / nitrosylsulfuric acid / acetic acid / 1 h / 0 °C

3: 45 percent / 2-mercaptoethanol / CHCl₃ / Ambient temperature

With nitrosylsulfuric acid; acetic acid; 2-hydroxyethanethiol; In chloroform; water; acetic acid;