Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

Base Information

Chemical Name:Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester
CAS No.:122763-78-4
Molecular Formula:C₂₁H₃₁O₇P
Molecular Weight:426.447
Hs Code.:

Synonyms:Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

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Chemical Property of Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

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Technology Process of Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

There total 11 articles about Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 122763-78-4
Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1) sodium naphthaleimide / 1) tetraethylene glycol dimethyl ether

With sodium naphthaleimide;
DOI:10.1021/jo00001a069

Reference yield:

: 464-49-3,68546-28-1
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

: 122763-78-4
Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / Br, HOAc / 6 h / 80 °C

2: 63 percent / Br₂, chlorosulfonic acid / 5 h / 25 °C

3: 60 percent / Zn, HOAc / 2 h / 25 °C

5: 1) sodium naphthaleimide / 1) tetraethylene glycol dimethyl ether

With chlorosulfonic acid; sodium naphthaleimide; bromine; bromine; acetic acid; zinc;
DOI:10.1021/jo00001a069

Reference yield:

: 10293-06-8
(1R)-3-endo-bromocamphor

: 122763-78-4
Acetic acid (R)-[(1S,6R)-2-(diethoxy-phosphoryloxy)-6-isopropenyl-3-methyl-cyclohex-2-enyl]-furan-2-yl-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / Br₂, chlorosulfonic acid / 5 h / 25 °C

2: 60 percent / Zn, HOAc / 2 h / 25 °C

4: 1) sodium naphthaleimide / 1) tetraethylene glycol dimethyl ether

With chlorosulfonic acid; sodium naphthaleimide; bromine; acetic acid; zinc;
DOI:10.1021/jo00001a069