3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

Base Information

Chemical Name:3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol
CAS No.:188399-45-3
Molecular Formula:C₄₀H₅₄O₉
Molecular Weight:678.863
Hs Code.:

3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

Synonyms:3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

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Chemical Property of 3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

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Technology Process of 3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

There total 4 articles about 3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 188399-44-2
C₄₇H₆₀O₉

: 188399-45-3
3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 6h; Ambient temperature;

Reference yield:

: 59291-87-1
1-benzyloxy-3,5-dihydroxybenzene

: 188399-45-3
3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / Cs₂CO₃ / dimethylformamide / 48 h / 90 °C

2: 89 percent / Cs₂CO₃ / dimethylformamide / 2.5 h / 100 °C

3: 85 percent / H₂ / 10percent Pd/C / ethanol; ethyl acetate / 6 h / Ambient temperature

With hydrogen; caesium carbonate; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 156276-65-2
Toluene-4-sulfonic acid (4S,5S)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 188399-45-3
3-[(4S,5S)-5-(4-tert-Butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-5-[(4R,5R)-5-(4-tert-butyl-phenoxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / Cs₂CO₃ / dimethylformamide / 48 h / 90 °C

2: 89 percent / Cs₂CO₃ / dimethylformamide / 2.5 h / 100 °C

3: 85 percent / H₂ / 10percent Pd/C / ethanol; ethyl acetate / 6 h / Ambient temperature

With hydrogen; caesium carbonate; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;