O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Base Information

Chemical Name:O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine
CAS No.:340283-86-5
Molecular Formula:C₁₈H₂₂F₃NOSi
Molecular Weight:353.459
Hs Code.:

Synonyms:O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

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Technology Process of O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

There total 2 articles about O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 19064-77-8,32213-72-2,85225-55-4
N-benzylidene-4-methylaniline oxide

: 340283-86-5
O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -30 - -20 ℃; for 48h;
DOI:10.1021/jo000685l

Reference yield:

: 5405-15-2
N-benzyl-N-(4-methylphenyl)amine

: 340283-86-5
O-trimethylsilyl (4-methylphenyl)[2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tungstate dihydrate; aq. H₂O₂ / methanol / 2 h / 0 °C

2: 84 percent / potassium t-butoxide / tetrahydrofuran / 48 h / -30 - -20 °C

With sodium tungstate; potassium tert-butylate; dihydrogen peroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo000685l