C₃₀H₄₉BrO₆S₄

Base Information

• Chemical Name: C₃₀H₄₉BrO₆S₄
• CAS No.: 359028-99-2
• Molecular Formula: C₃₀H₄₉BrO₆S₄
• Molecular Weight: 713.883
• Mol file: 359028-99-2.mol

Synonyms:C₃₀H₄₉BrO₆S₄

Chemical Property of C₃₀H₄₉BrO₆S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₉BrO₆S₄

There total 2 articles about C₃₀H₄₉BrO₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → C30H49BrO6S4 (359028-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: p-TsOH*H₂O / CH₂Cl₂ / 4 h

2: 70 percent / NaH (60 percent) / tetrahydrofuran / 20 h / Heating

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/hc.1044

Reference yield:

2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol (5244-34-8) → C30H49BrO6S4 (359028-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: p-TsOH*H₂O / CH₂Cl₂ / 4 h

2: 70 percent / NaH (60 percent) / tetrahydrofuran / 20 h / Heating

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/hc.1044

Reference yield: 74.0%

C30H49BrO6S4 (359028-99-2) → 2-{2-[2-(2-bromo-3-{2-[2-(2-hydroxy-ethylsulfanyl)-ethylsulfanyl]-ethoxymethyl}-benzyloxy)-ethylsulfanyl]-ethylsulfanyl}-ethanol (359029-00-8)

Guidance literature:

With hydrogenchloride; methanol; In tetrahydrofuran; chloroform; at 20 ℃; for 39h;

DOI:10.1002/hc.1044

upstream raw materials:

3,4-dihydro-2H-pyran

2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol

Downstream raw materials:

2-{2-[2-(2-bromo-3-{2-[2-(2-hydroxy-ethylsulfanyl)-ethylsulfanyl]-ethoxymethyl}-benzyloxy)-ethylsulfanyl]-ethylsulfanyl}-ethanol

Refernces