9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

Base Information

Chemical Name:9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester
CAS No.:78939-38-5
Molecular Formula:C₁₈H₂₀N₂O₈
Molecular Weight:392.365
Hs Code.:

Synonyms:9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

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Chemical Property of 9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

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Technology Process of 9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

There total 1 articles about 9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38256-25-6
dimethyl (E)-2-oxoglutaconate

: 78939-36-3
6-amino-5-methoxy-2-methoxycarbonylindole

: 78939-38-5
9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

Guidance literature:: In dichloromethane; at 25 ℃; for 16h;

Reference yield:

: 78939-38-5
9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

: 72909-34-3
pyrroloquinoline quinone

Guidance literature:: Multi-step reaction with 4 steps

1: dry hydrogen chloride / CH₂Cl₂ / 10 h

2: 60 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.17 h / 0 °C

3: 92 percent / p-tuluenesulfonic acid / methanol / 4 h / Heating

4: 98 percent / 0.5 M K₂CO₃ / H₂O / 4 h / 85 °C

With hydrogenchloride; ammonium cerium(IV) nitrate; potassium carbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja00408a067

Reference yield:

: 78939-38-5
9-Hydroxy-5-methoxy-6,7,8,9-tetrahydro-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylic acid trimethyl ester

: 73030-04-3
4,5-dihydro-5-hydroxy-4-oxo-5-(2-oxopropyl)-1H-pyrrolo<2,3-f>quinoline-2,7,9-tricarboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: dry hydrogen chloride / CH₂Cl₂ / 10 h

2: 60 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.17 h / 0 °C

3: 92 percent / p-tuluenesulfonic acid / methanol / 4 h / Heating

4: 98 percent / 0.5 M K₂CO₃ / H₂O / 4 h / 85 °C

5: NH₄OH / H₂O / 30 h / 23 °C

With hydrogenchloride; ammonium hydroxide; ammonium cerium(IV) nitrate; potassium carbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja00408a067