4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

Base Information

Chemical Name:4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol
CAS No.:1351592-67-0
Molecular Formula:C₂₂H₂₂F₃NO₅
Molecular Weight:437.416
Hs Code.:

Synonyms:4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

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Chemical Property of 4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

Chemical Property:

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Technology Process of 4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

There total 3 articles about 4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351592-04-5
2-((2,2-diethoxyethylamino)methyl)-6-ethoxyphenol

: 501699-84-9
3,5-Dimethoxy-4-(2,2,2-trifluoroethoxy)benzaldehyd

: 1351592-67-0
4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

Guidance literature:: 2-((2,2-diethoxyethylamino)methyl)-6-ethoxyphenol; 3,5-Dimethoxy-4-(2,2,2-trifluoroethoxy)benzaldehyd; With hydrogenchloride; In ethanol; water; at 90 ℃; for 0.416667h;

With ammonium hydroxide;

Reference yield:

: 134-96-3
syringic aldehyde

: 1351592-67-0
4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 150 °C / Microwave irradiation

2: hydrogenchloride / ethanol; water / 0.42 h / 90 °C

With hydrogenchloride; caesium carbonate; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1351592-03-4
(E)-2-((2,2-diethoxyethylimino)methyl)-6-ethoxyrhenol

: 1351592-67-0
4-(3,5-dimethoxy-4-(2,2,2-trifluoroethoxy)benzyl)-7-ethoxyisoquinolin-8-ol

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; sodium tetrahydroborate / 1 h / 100 °C / Inert atmosphere

2: hydrogenchloride / ethanol; water / 0.42 h / 90 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; In ethanol; water;