C₃₇H₄₈N₄O₁₄S

Base Information

• Chemical Name: C₃₇H₄₈N₄O₁₄S
• CAS No.: 1337988-14-3
• Molecular Formula: C₃₇H₄₈N₄O₁₄S
• Molecular Weight: 804.873
• Mol file: 1337988-14-3.mol

Synonyms:C₃₇H₄₈N₄O₁₄S

Chemical Property of C₃₇H₄₈N₄O₁₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₄₈N₄O₁₄S

There total 3 articles about C₃₇H₄₈N₄O₁₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C2HF3O2*C33H41N3O11 (1337987-98-0) + 3-carboxypropane sulfonamide (175476-52-5) → C37H48N4O14S (1337988-14-3)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1016/j.bmcl.2011.08.035

Reference yield:

C33H41N3O11 (1337987-97-9) → C37H48N4O14S (1337988-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water; acetonitrile

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In water; acetonitrile;

DOI:10.1016/j.bmcl.2011.08.035

Reference yield:

novobiocin (303-81-1,107781-69-1) → C37H48N4O14S (1337988-14-3)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid / tetrahydrofuran / 2 h / 120 °C / Microwave irradiation

2: water; acetonitrile

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetonitrile; 1: Mannich reaction;

DOI:10.1016/j.bmcl.2011.08.035

upstream raw materials:

C₂HF₃O₂*C₃₃H₄₁N₃O₁₁

3-carboxypropane sulfonamide

C₃₃H₄₁N₃O₁₁

novobiocin