2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

Base Information

Chemical Name:2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane
CAS No.:1429347-67-0
Molecular Formula:C₂₁H₃₉NO₄Si₂
Molecular Weight:425.716
Hs Code.:

Synonyms:2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

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Technology Process of 2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

There total 1 articles about 2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 91748-03-7
1,3-dihydroxy-2-(4-nitrophenyl)propane

: 1429347-67-0
2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 1429347-67-0
2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

: 1429347-68-1
4-(2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecan-6-yl)aniline

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; under 7500.75 Torr;

Reference yield:

: 1429347-67-0
2,2,3,3,9,9,10,10-octamethyl-6-(4-nitrophenyl)-4,8-dioxa-3,9-disilaundecane

: N-(4-(1,3-dihydroxypropan-2-yl)phenyl)-4-(((3,5-dimethylisoxazol-4-yl)oxy)methyl)-N-isobutylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 20 °C / 7500.75 Torr

2: potassium iodide; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / water / 1.5 h / 150 °C / Microwave irradiation; Sealed tube

3: pyridine

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

With pyridine; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium iodide; In tetrahydrofuran; ethanol; water;