potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

Base Information

Chemical Name:potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate
CAS No.:1402242-83-4
Molecular Formula:C₁₀H₆BF₆N₂*K
Molecular Weight:318.071
Hs Code.:

Synonyms:potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

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Chemical Property of potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

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Technology Process of potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

There total 3 articles about potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1402242-65-2
potassium trifluoro(3-oxo-3-(4-(trifluoromethyl)phenyl)prop-1-ynyl)borate

: 1402242-83-4
potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

Guidance literature:: With hydrazine hydrate; In ethanol; at 20 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol302418b

Reference yield:

: 1402242-59-4
potassium trifluoro(3-hydroxy-3-(4-(trifluoromethyl)phenyl)prop-1-ynyl)borate

: 1402242-83-4
potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / acetone / 2 h / 20 °C / Inert atmosphere

2: hydrazine hydrate / ethanol / 2 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; hydrazine hydrate; In ethanol; acetone;
DOI:10.1021/ol302418b

Reference yield:

: 83494-26-2
α-ethynyl-4-(trifluoromethyl)-benzenemethanol

: 1402242-83-4
potassium trifluoro(3-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-yl)borate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - -20 °C / Inert atmosphere

1.3: 1 h / -20 - 20 °C / Inert atmosphere

2.1: manganese(IV) oxide / acetone / 2 h / 20 °C / Inert atmosphere

3.1: hydrazine hydrate / ethanol / 2 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; n-butyllithium; hydrazine hydrate; In tetrahydrofuran; ethanol; hexane; acetone;
DOI:10.1021/ol302418b