(2,3-diphenyloxiran-2-yl)methanol

Base Information

• Chemical Name: (2,3-diphenyloxiran-2-yl)methanol
• CAS No.: 503625-08-9
• Molecular Formula: C₁₅H₁₄O₂
• Molecular Weight: 226.275
• Mol file: 503625-08-9.mol

Synonyms:(2,3-diphenyloxiran-2-yl)methanol

Chemical Property of (2,3-diphenyloxiran-2-yl)methanol

Chemical Property:

Purity/Quality:

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Technology Process of (2,3-diphenyloxiran-2-yl)methanol

There total 1 articles about (2,3-diphenyloxiran-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

α-phenylcinnamyl alcohol (22835-64-9) → (2,3-diphenyloxiran-2-yl)methanol (503625-08-9)

Guidance literature:

With 1-phenylethyl hydroperoxide; dimethyl Isophthalate; K₁₂[ZnW(VO)2(ZnW₉O₃₄)2]*30H₂O; In 1,2-dichloro-ethane; at 20 ℃; for 24h;

DOI:10.1021/ol027498p

Reference yield: 82.0%

(2,3-diphenyloxiran-2-yl)methanol (503625-08-9) + aniline (62-53-3) → erythro-2,3-diphenyl-3-(phenylamino)propane-1,2-diol

Guidance literature:

With tungsten hexa-ethoxide; In acetonitrile; at 55 ℃; for 24h; stereospecific reaction;

DOI:10.1021/ja5029809

Reference yield: 80.0%

(2,3-diphenyloxiran-2-yl)methanol (503625-08-9) + aniline (62-53-3) → 2,3-diphenyl-3-(phenylamino)propane-1,2-diol

Guidance literature:

With magnesium chloride; In N,N-dimethyl-formamide; at 20 - 80 ℃; Sealed tube;

DOI:10.1016/j.tetlet.2021.153013

upstream raw materials:

α-phenylcinnamyl alcohol