2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

Base Information

Chemical Name:2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione
CAS No.:1617512-27-2
Molecular Formula:C₂₁H₁₇NO₃
Molecular Weight:331.371
Hs Code.:

Synonyms:2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

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Chemical Property of 2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

Chemical Property:

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Technology Process of 2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

There total 4 articles about 2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1617512-12-5
2-chloromethyl-3-methylnaphtho[1,2-b]furan-4,5-dione

: 108-44-1
1-amino-3-methylbenzene

: 1617512-27-2
2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 55 ℃; for 2h;
DOI:10.1016/j.ejmech.2014.05.041

Reference yield:

: 1617512-11-4
3-methyl-2-morpholino-5-hydroxy-2,3-dihydronaphtho[1,2-b]furan

: 1617512-27-2
2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / tetrahydrofuran; water / 2 h / 75 °C

2: potassium dihydrogenphosphate / water; acetone / 12 h / 20 °C

3: hydrogenchloride / ethyl acetate / 5 h / 45 - 50 °C

4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 2 h / 55 °C

With hydrogenchloride; potassium dihydrogenphosphate; potassium carbonate; potassium iodide; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2014.05.041

Reference yield:

: 52422-61-4
3-methyl-4,5-dihydronaphtho<1.2-b>furan-4,5-dione

: 1617512-27-2
2-(((3-methylphenyl)amino)methyl)-3-methylnaphtho[1,2-b]furan-4,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethyl acetate / 5 h / 45 - 50 °C

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 2 h / 55 °C

With hydrogenchloride; potassium carbonate; potassium iodide; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.05.041