N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

Base Information

Chemical Name:N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide
CAS No.:1623775-25-6
Molecular Formula:C₂₅H₂₄N₄O
Molecular Weight:396.492
Hs Code.:

Synonyms:N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

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Chemical Property of N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

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Technology Process of N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

There total 8 articles about N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1623775-05-2
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide

: 100-58-3
phenylmagnesium bromide

: 1623775-25-6
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

Guidance literature:: N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide; phenylmagnesium bromide; With iron(III) chloride; N,N,N,N,-tetramethylethylenediamine; zinc dibromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

With 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With 1,2-dichloro-2-methylpropane; In tetrahydrofuran; at 55 ℃; for 48h;
DOI:10.1002/anie.201311024

Reference yield: 66.0%

: 1623775-05-2
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide

: 111409-79-1
1-bromo-2-(triisopropylsilyl)acetylene

: 100-58-3
phenylmagnesium bromide

: 1623775-25-6
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

: C₄₁H₆₀N₄OSi₂

: N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)propan-2-yl]-2[(triisopropylsilyl)ethynyl]benzamide

Guidance literature:: N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide; phenylmagnesium bromide; With dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc; cis-1,2-bis-(diphenylphosphino)ethene; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

1-bromo-2-(triisopropylsilyl)acetylene; With iron(III)-acetylacetonate; In tetrahydrofuran; at 65 ℃; for 1h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201700587

Reference yield:

: C₁₉H₁₅⁽²⁾H₅N₄O

: 1623775-05-2
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide

: 100-58-3
phenylmagnesium bromide

: 1623775-38-1
C₂₅H₂₀⁽²⁾H₄N₄O

: 1623775-25-6
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-[1,1'-biphenyl]-2-carboxamide

Guidance literature:: C₁₉H₁₅⁽²⁾H₅N₄O; N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)benzamide; phenylmagnesium bromide; With N,N,N,N,-tetramethylethylenediamine; zinc dibromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

With iron(III) chloride; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With 1,2-dichloro-2-methylpropane; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1002/anie.201311024