C₁₅H₁₆O

Base Information

• Chemical Name: C₁₅H₁₆O
• CAS No.: 1432498-64-0
• Molecular Formula: C₁₅H₁₆O
• Molecular Weight: 212.291
• Mol file: 1432498-64-0.mol

Synonyms:C₁₅H₁₆O

Chemical Property of C₁₅H₁₆O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₆O

There total 4 articles about C₁₅H₁₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C15H18O (1432499-19-8) → C15H16O (1432498-64-0)

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja4025963

Reference yield:

2-phenylhex-5-enoic acid (156297-00-6) → C15H16O (1432498-64-0)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: zinc; ammonium chloride / toluene; water; tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; pyridinium chlorochromate; zinc; In tetrahydrofuran; dichloromethane; water; toluene;

DOI:10.1021/ja4025963

Reference yield:

2-phenyl-5-hexen-1-ol (177037-77-3) → C15H16O (1432498-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: zinc; ammonium chloride / toluene; water; tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; pyridinium chlorochromate; zinc; In tetrahydrofuran; dichloromethane; water; toluene;

DOI:10.1021/ja4025963

upstream raw materials:

2-phenylhex-5-enoic acid

2-phenyl-5-hexen-1-ol

2-phenyl-5-hexenal

C₁₅H₁₈O