N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

Base Information

Chemical Name:N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide
CAS No.:1043922-68-4
Molecular Formula:C₂₆H₂₇N₃O₃
Molecular Weight:429.519
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

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Chemical Property of N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

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Technology Process of N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

There total 2 articles about N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 122-78-1
phenylacetaldehyde

: 81378-80-5
(S)-benzyl (1-(1-methylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

: 1043922-68-4
N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1002/anie.200705858

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 1043922-68-4
N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 °C / Inert atmosphere

1.2: 24 h / -25 - 25 °C

2.1: magnesium sulfate / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

With 4-methyl-morpholine; magnesium sulfate; isobutyl chloroformate; In tetrahydrofuran;
DOI:10.1002/chem.201103322

Reference yield: 66.0%

: 1043922-68-4
N-(benzyloxycarbonyl)phenylalanine 1-methyl-2-phenylethylidenehydrazide

: 1043922-69-5
(S)-benzyl (1-(1-methyl-2-phenethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: With dimethylamine borane; toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1002/anie.200705858