ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

Base Information

Chemical Name:ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate
CAS No.:1454797-90-0
Molecular Formula:C₄₅H₄₂O₆
Molecular Weight:678.825
Hs Code.:

Synonyms:ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

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Chemical Property of ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

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Technology Process of ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

There total 4 articles about ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: C₂₇H₂₃BrO₂

: 50463-56-4
4-benzyloxy-3-methoxyphenylacetic acid ethyl ester

: 1454797-90-0
ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

Guidance literature:: 4-benzyloxy-3-methoxyphenylacetic acid ethyl ester; With diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

C₂₇H₂₃BrO₂; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.07.058

Reference yield:

: 536975-31-2
bis(4-benzyloxyphenyl)methanol

: 1454797-90-0
ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Acetyl bromide / benzene / 5 h / 30 °C / Inert atmosphere

2.1: diisopropylamine / hexane; tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

With Acetyl bromide; diisopropylamine; In tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.bmcl.2013.07.058

Reference yield:

: 6793-92-6
p-benzyloxyphenylbromide

: 1454797-90-0
ethyl 2-(4-(benzyloxy)-3-methoxyphenyl)-3,3-bis(4-(benzyloxy)phenyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.58 h / -78 °C / Inert atmosphere

2.1: Acetyl bromide / benzene / 5 h / 30 °C / Inert atmosphere

3.1: diisopropylamine / hexane; tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

With n-butyllithium; Acetyl bromide; diisopropylamine; In tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.bmcl.2013.07.058