11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

Base Information

Chemical Name:11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one
CAS No.:74780-72-6
Molecular Formula:C₁₉H₁₆ClNO₂
Molecular Weight:325.795
Hs Code.:

11-<trans-3-(4-chlorophenyl)-3-oxoprop-1-enyl>-11-endo-11-azatricyclo<5.3.1.0<sup>2,6</sup>>undeca-3,9-dien-8-one

Synonyms:11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

Suppliers and Price of 11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

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Technology Process of 11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

There total 6 articles about 11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 74793-93-4
1--3-hydroxypyrimidinium chloride

: 74780-72-6
11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

: 74780-71-5
7--exo-7-azabicyclo<4.3.1.1^2,5>undeca-3,8-dien-10-one

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;

Reference yield: 23.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 74780-48-6
1--3-oxidopyridinium

: 74780-72-6
11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

: 74780-71-5
7--exo-7-azabicyclo<4.3.1.1^2,5>undeca-3,8-dien-10-one

Guidance literature:: With hydroquinone; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1039/P19800000362

Reference yield:

: 15724-88-6
trans-1-(4-chlorophenyl)-3-chloroprop-2-en-1-one

: 74780-72-6
11--11-endo-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / triethylamine / CH₂Cl₂ / 24 h / 20 °C

With triethylamine; In dichloromethane; 2: Katritzky's cycloaddition;