(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

Base Information

Chemical Name:(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum
CAS No.:126949-74-4
Molecular Formula:C₃₄H₅₆MoN₂
Molecular Weight:588.772
Hs Code.:

(2,6-diisopropylphenylimido)2(CH<sub>2</sub>C-tBu)2 molybdenum

Synonyms:(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

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Chemical Property of (2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

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Technology Process of (2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

There total 5 articles about (2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: bis((2,6-diisopropylphenyl)imido)dichloromolybdenum(VI)-tetrahydrofuran

: 7412-67-1
neopentyl lithium

: 126949-74-4
(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

Guidance literature:: In pentane; byproducts: LiCl; Ar, stirred for 12 h; evapd.; recrystd. (pentane); elem. anal.;
DOI:10.1021/om00055a065

Reference yield: 80.0%

: 126949-60-8
Mo(N-2,6-Pr(i)2C₆H₃)2Cl₂ * dme

: 7412-67-1
neopentyl lithium

: 126949-74-4
(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

Guidance literature:: In diethyl ether; at -78 - 23 ℃; for 7.5h; Schlenk technique;
DOI:10.1021/acs.organomet.7b00115

Reference yield: 70.0%

: MoCl2(N(2,6-i-Pr2C6H3))2(1,2-dimethoxyethane)

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 126949-74-4
(2,6-diisopropylphenylimido)2(CH₂C-tBu)2 molybdenum

Guidance literature:: In diethyl ether; byproducts: MgCl2, 1,2-dimethoxyethane; soln. of ClMgCH2C(CH3)3 is added to soln. of Mo(NC6H3(CH(CH3)2)2)(DME)Cl2 in Et2O at -30°C, mixt. is allowed to warm to 25°C and is stirred for 3 h,; filtn. through Celite, filtrate is concentrated in vac. and kept at -40°C, elem. anal.;
DOI:10.1021/ja00166a023