5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt

Base Information

• Chemical Name: 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt
• CAS No.: 82902-27-0
• Molecular Formula: C₆H₁₅N*C₄₄H₃₉ClN₅O₉P
• Molecular Weight: 949.44

Synonyms:5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt

Chemical Property of 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt

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Technology Process of 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt

There total 1 articles about 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1,2,4]Triazol-1-yl-phosphonic acid (2R,3S,5R)-5-(6-benzyloxycarbonylamino-purin-9-yl)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester (82902-25-8) + triethylamine (121-44-8) → 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt (82902-27-0)

Guidance literature:

With water; Yield given;

DOI:10.1021/ja00385a026

Reference yield: 82.0%

6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate) (82892-68-0) + 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt (82902-27-0) → C78H69Cl2N11O17P2 (82902-34-9)

Guidance literature:

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole;

DOI:10.1021/ja00385a026

Reference yield: 78.0%

3'-O-levulinyl-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine (82892-69-1) + 5'-O-(methoxytrityl)-6-N-(benzyloxycarbonyl)-2'-deoxyadenosine 3'-O-(2-chlorophenyl phosphate) triethylammonium salt (82902-27-0) → C74H68ClN10O16P (82902-35-0)

Guidance literature:

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole;

DOI:10.1021/ja00385a026

upstream raw materials:

[1,2,4]Triazol-1-yl-phosphonic acid (2R,3S,5R)-5-(6-benzyloxycarbonylamino-purin-9-yl)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

triethylamine

Downstream raw materials:

C₆₉H₆₂ClN₁₀O₁₄P

C₆₉H₆₂ClN₁₀O₁₄P

C₇₄H₆₈ClN₁₀O₁₆P

C₇₈H₆₉Cl₂N₁₁O₁₇P₂

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