6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

Base Information

Chemical Name:6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)
CAS No.:82892-68-0
Molecular Formula:C₃₄H₃₂ClN₆O₉P
Molecular Weight:735.09
Hs Code.:

Synonyms:6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

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Chemical Property of 6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

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Technology Process of 6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

There total 3 articles about 6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 82902-29-2
5'-O-(methoxytrityl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

: 82892-68-0
6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

Guidance literature:: With benzenesulfonic acid;
DOI:10.1021/ja00385a026

Reference yield:

: 82892-61-3
5'-O-(methoxytrityl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

: 82892-68-0
6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triazole, triethylamine / 1.) THF

2: 85 percent / 2percent benzenesulfonic acid

With 1,2,3-triazole; triethylamine; benzenesulfonic acid;
DOI:10.1021/ja00385a026

Reference yield:

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 82892-68-0
6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triazole, triethylamine / 1.) THF

2: 85 percent / 2percent benzenesulfonic acid

With 1,2,3-triazole; triethylamine; benzenesulfonic acid;
DOI:10.1021/ja00385a026