Technology Process of C39H52N5O6P
There total 4 articles about C39H52N5O6P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
aq. phosphate buffer; N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
pH=7.4;
DOI:10.1021/ol3022484
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0.17 h / 20 °C
1.2: 1 h / 20 °C
2.1: ammonium chloride; sulfuric acid / ethyl acetate / 0.5 h / 20 °C
3.1: triethylamine / dichloromethane / 3 h / 0 °C
4.1: N,N-dimethyl-formamide; aq. phosphate buffer / 0.5 h / 20 °C / pH 7.4
With
dmap; sulfuric acid; ammonium chloride; triethylamine; dicyclohexyl-carbodiimide;
In
aq. phosphate buffer; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
4.1: |Staudinger Azide Reduction;
DOI:10.1021/ol3022484
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 3 h / 0 °C
2: N,N-dimethyl-formamide; aq. phosphate buffer / 0.5 h / 20 °C / pH 7.4
With
triethylamine;
In
aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide;
2: |Staudinger Azide Reduction;
DOI:10.1021/ol3022484