1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) 2-phenyl ester, (S)-

Base Information

Chemical Name:1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) 2-phenyl ester, (S)-
CAS No.:64411-39-8
Molecular Formula:C16H21NO4
Molecular Weight:291.347
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) 2-phenyl ester, (S)-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) 2-phenyl ester, (S)-

There total 10 articles about 1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) 2-phenyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 108-95-2,27073-41-2
phenol

: 64411-39-8
1-tert-butyl 2-phenyl pyrrolidine-1,2-dicarboxylate

Guidance literature:: 1-(tert-butoxycarbonyl)-L-proline; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.166667h;

phenol; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ol3022484

Reference yield: 80.0%

: 15761-39-4,59433-50-0
N-tert-butoxycarbonyl-proline

: 108-95-2,27073-41-2
phenol

: 64411-39-8
1-(tert-butyl) 2-phenyl pyrrolidine-1,2-dicarboxylate

Guidance literature:: N-tert-butoxycarbonyl-proline; With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

phenol; In dichloromethane; at 20 ℃; for 24h;

Reference yield: 57.0%

: 86953-79-9
tert-butyl pyrrolidine-1-carboxylate

: 1885-14-9
phenyl chloroformate

: 64411-39-8
1-(tert-butyl) 2-phenyl pyrrolidine-1,2-dicarboxylate

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; sodium tungstate (VI) dihydrate; phosphate potassium salt; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine; In benzene; at 40 ℃; for 48h; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/jacs.8b09191