5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

Base Information

• Chemical Name: 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine
• CAS No.: 1031443-55-6
• Molecular Formula: C₁₄H₁₅BF₂I₂N₂
• Molecular Weight: 513.903

Synonyms:5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

Chemical Property of 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

5,5-Difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4l4,5l4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

There total 7 articles about 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4,4-difluoro-1,3,5,7,8-pentamethyl-4-bora-3a,4a-diaza-s-indecene (121207-31-6) → 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ4,5λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (1031443-55-6)

Guidance literature:

With N-iodo-succinimide; In dichloromethane; at 25 ℃; for 12h;

DOI:10.1039/c3ob40213d

Reference yield: 85.0%

N-iodo-succinimide (516-12-1) + 4,4-difluoro-1,3,5,7,8-pentamethyl-4-bora-3a,4a-diaza-s-indecene (121207-31-6) → 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ4,5λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (1031443-55-6)

Guidance literature:

In dichloromethane; at 28 ℃; for 12h; Schlenk technique; Inert atmosphere; Darkness;

DOI:10.1039/c6nj03033e

Reference yield: 84.0%

iodine (7553-56-2,12190-71-5,8031-47-8) + 4,4-difluoro-1,3,5,7,8-pentamethyl-4-bora-3a,4a-diaza-s-indecene (121207-31-6) → 5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ4,5λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (1031443-55-6)

Guidance literature:

With iodic acid; In ethanol; for 16h; Inert atmosphere;

DOI:10.1002/ejoc.201601372

upstream raw materials:

4,4-difluoro-1,3,5,7,8-pentamethyl-4-bora-3a,4a-diaza-s-indecene

2,4-dimethyl-1H-pyrrole

iodic acid

N-iodo-succinimide

Downstream raw materials:

C₄₆H₅₉BF₂N₄

4,4-difluoro-1,3,5,7,8-pentamethyl-2,6-bis(p-tolylethynyl)-4-bora-3a,4a-diaza-s-indacene

4,4-bis(p-tolylethynyl)-1,3,5,7,8-pentamethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

C₃₂H₂₇BF₂N₂O₂

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