[N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃

Base Information

• Chemical Name: [N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃
• CAS No.: 872513-68-3
• Molecular Formula: C₂₇H₂₉Cl₄NOSTi
• Molecular Weight: 605.291

Synonyms:[N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃

Chemical Property of [N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃

Chemical Property:

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Technology Process of [N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃

There total 1 articles about [N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

((CH3)3C)2C6H2(OH)CHNC6H4SC6H4Cl (872513-61-6) + titanium tetrachloride (7550-45-0) → [N-(3,5-di-tert-butylsalicylidene)-2-(3-chlorophenylsulfanyl)anilinato]Ti(IV)Cl3 (872513-68-3)

Guidance literature:

With KH; In toluene; under Ar atm. to suspn. KH in THF at -78°C soln. ligand in THF was added, allowed to warm to room temp., stirred for 2 h, solvent was removed in vacuo, residue was dissolved in toluene, soln. TiCl4 in toluene was added at r.t., stirred overnight; soln. was filtered, ppt. was washed with CH2Cl2, combined filtrates wereconcd. in vacuo and cooled to -30°C overnight, ppt. was dried in vacuo; elem. anal.;

DOI:10.1021/om060062j

upstream raw materials:

((CH₃)3C)2C₆H₂(OH)CHNC₆H₄SC₆H₄Cl

titanium tetrachloride

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