(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

Base Information

Chemical Name:(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide
CAS No.:925460-48-6
Molecular Formula:C₂₆H₂₇N₃O₈S
Molecular Weight:541.582
Hs Code.:

Synonyms:(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

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Technology Process of (Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

There total 1 articles about (Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 126029-41-2
(2Z)-5-(benzyloxy)pent-2-en-1-ol

: N-(4-methoxybenzyl)-2,4-dinitro-benzenesulfonamide

: 925460-48-6
(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jo062178v

Reference yield: 76.0%

: 925460-48-6
(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

: 925460-49-7
(Z)-N-(5-benzyloxy-pent-2-enyl)-(4-methoxy-benzyl)-amine

Guidance literature:: With mercaptoacetic acid; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo062178v

Reference yield:

: 925460-48-6
(Z)-N-(5-benzyloxy-pent-2-enyl)-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

: 2-(5-benzyloxy-pent-2-enylamino)-3-(4-methoxy-phenyl)-N,N-dimethyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / Et₃N; mercaptoacetic acid / CH₂Cl₂ / 20 °C

2: 94 percent / K₂CO₃ / acetonitrile / 3.5 h / 20 °C

3: 17 percent / Et₃N; (4R,5R)-2-Br-1,3-ditosyl-4,5-diphenyl-1,3,2-diazaborolidine / CH₂Cl₂ / 72 h / 20 °C

With (4R,5R)-2-bromo-1,3-bis[(4-methylphenyl)sulfonyl]-4,5-diphenyl-1,3,2-diazaborolidine; potassium carbonate; mercaptoacetic acid; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jo062178v