Technology Process of 2-Penten-1-ol, 5-(phenylmethoxy)-, (2Z)-
There total 9 articles about 2-Penten-1-ol, 5-(phenylmethoxy)-, (2Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
Lindlar's catalyst;
In
ethyl acetate;
at 20 ℃;
for 6h;
atmospheric pressure;
DOI:10.1021/ja0469075
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 66 percent / PPh3; I2; imidazole / benzene / 2 h / 0 °C
2.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
2.2: 84 percent / HMPA / tetrahydrofuran; hexane / -78 °C
3.1: 76 percent / tetrabutylammonium fluoride / tetrahydrofuran
4.1: 98 percent / H2 / Lindlar's catalyst / ethyl acetate / 6 h / 20 °C / 760 Torr
With
1H-imidazole; n-butyllithium; tetrabutyl ammonium fluoride; hydrogen; iodine; triphenylphosphine;
Lindlar's catalyst;
In
tetrahydrofuran; hexane; ethyl acetate; benzene;
DOI:10.1021/ja065833p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 84 percent / HMPA / tetrahydrofuran; hexane / -78 °C
2.1: 76 percent / tetrabutylammonium fluoride / tetrahydrofuran
3.1: 98 percent / H2 / Lindlar's catalyst / ethyl acetate / 6 h / 20 °C / 760 Torr
With
n-butyllithium; tetrabutyl ammonium fluoride; hydrogen;
Lindlar's catalyst;
In
tetrahydrofuran; hexane; ethyl acetate;
DOI:10.1021/ja065833p
